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Synthesis of α-aminophosphonates using solvate ionic liquids

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journal contribution
posted on 2017-01-01, 00:00 authored by Daniel Eyckens, Luke HendersonLuke Henderson
A range of α-aminophosphonates were accessed in high yields and very rapidly, using solvate ionic liquids as the reaction media. Reactions typically required less than 10 minutes to go to completion and precipitation of these products into water excludes the use of traditional work up procedures, giving the products in very high crude purity. Excellent functional group tolerance for both the aldehyde and amine reaction partners was observed, and a range of bis-aminophosphonates derived from aromatic diamines were also accessed in high yield and purity.

History

Journal

RSC advances

Volume

7

Issue

45

Pagination

27900 - 27904

Publisher

Royal Society of Chemistry

Location

Cambridge, Eng.

eISSN

2046-2069

Language

eng

Publication classification

C1 Refereed article in a scholarly journal

Copyright notice

2017, The Royal Society of Chemistry